Izinyathelo Zokuqapha Zokusebenzisa Ama-Hastelloy Alloy High-Pressure Reactors

1. Indawo Yokufaka

II-HastelloyAlloy High Ingcindezi Rumlingisikufanele ifakwe egumbini lokusebenza elinomfutho ophezulu elihlangabezana nezidingo ezingaqhumi. Uma kusetshenziswa ama-reactor amaningi e-Hastelloy, kufanele abekwe ngokwehlukana, lapho ama-reactor amabili ehlukaniswe ngodonga oluphephile olungaqhumi. Kunoma yiziphi izindlela eziholela ngaphandle, qiniseka ukuthi imishini inomoya omuhle lapho kukhona izinto eziqhumayo.

2. Izinto Okumelwe Uzicabangele Ngokushisa

Uma kusetshenziswa ukushisa ngogesi kawoyela oshisayo, qiniseka ukuthi uthenga uhlobo olufanele lwamafutha okushisa ngokusekelwe ekushiseni okusebenzayo.

3. Ukuvala i-Reactor

Umzimba we-reactor kanye nesembozo kumele kwenze ukuxhumana okuqondile ne-gasket noma nezindawo zokuvala ezi-conical nezi-arcuate. Ukuqinisa i-nut eyinhloko kuyayicindezela ndawonye ukuze kufezwe ukuvala okusebenzayo. Uma iqiniswa, i-nut kufanele iguqulwe ngokulinganayo nangokuhamba kancane ngezigaba eziningana ukuqinisekisa ukucindezela okulinganayo nokuvimbela isembozo ukuthi singatsheki, ngaleyo ndlela kuqinisekiswe ukuvala okufanele.

4. Ukufakwa kweValve kanye neGauge

Faka ama-valve, ama-pressure gauge, nama-valve okuphepha ngokuqinisa amantongomane afanele ukuze kutholakale isivalo. Izindawo zokuvala ezigobile kuzo zombili izinhlangothi zokuxhuma akumele zijikeleze ngokuhambisana. Ngesikhathi sokuhlanganiswa, wonke ama-joint anezintambo kumele agcotshwe—kungaba ngesithambisi esifanele noma ingxube kawoyela we-graphite—ukuvimbela ukugabha.

5. Inqubo Yokupholisa

Ukuze kuphole, amanzi angajikeleziswa ngamakhoyili okupholisa angaphakathi. Ukupholisa okusheshayo akuvunyelwe ukugwema ukucindezeleka okukhulu kokushisa okungase kuqhekeze amakhoyili okupholisa kanye nomzimba we-reactor. Ngesikhathi sokusebenza, uma izinga lokushisa le-reactor lidlula i-100°C, amanzi okupholisa kufanele ajikelezwe ngejakethi yamanzi phakathi kwe-magnetic stirrer kanye nesembozo se-reactor ukuqinisekisa ukuthi izinga lokushisa lamanzi lihlala lingaphansi kuka-35°C, okusiza ukuvimbela ukukhishwa kwamandla kagesi.

6. Izinqubo Ngemva Kokusabela

Ngemva kokuthi ukusabela sekuqediwe, qala uvumele i-reactor ukuthi iphole, bese ukhulula igesi yangaphakathi ngepayipi ukuze unciphise ukucindezela komoya. Ungawuqaqi i-reactor ngenkathi isacindezelwe. Khulula amabhawodi amakhulu namantongomane ngokulinganayo, uwasuse, bese uvula ngokucophelela bese ususa isembozo, usibeke esitendini.

Ukugcinwa Nokuhlanza

Ngemva komsebenzi ngamunye, hlanza i-reactor ngoketshezi lokuhlanza olufanele ukuvimbela ukugqwala kwezinto eziyinhloko. Susa noma yiziphi izinsalela emzimbeni we-reactor kanye nezindawo zokuvala. Gcina imishini ihlanzekile njalo.

Ukuze uthole imininingwane eyengeziwe mayelana nama-micro-reactors kanye ne-laboratory-scaleHigh PqinisekisaRabadlali, zizwe ukhululekileCxhumana nathi.